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Department of process engineering U218

Direct ohmic heating - instructions

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Measurement procedure

Simplest experiment with tap water.
  • Switch on PC, and power supply of transducers. Start program PCL818 or OHMICAS (time step 1 s, 9 channels).
  • Set 3-way cock K1 to position 1 (K1/1), and open valve V2 (filling water). Check water level visually (glass gauge) and on display (channel 8). After filling close V2.
  • Set cock K3/1 and K1/4. Water flows to the outlet. Estimate the flowrate (using F10 in the OHMICAS program). Adjust the flowrate by valve V1.
  • Switch on heating and adjust electrical power (check overloading on the control panel). Wait until the steady state is achieved.
  • Precise value of flowrate can be obtained by measurement of volume at a time interval. Use stop-watch and calibrated vessel (2 to 8 litres).

Photogallery

Filling the tank by water - Check the level of water by electronic gauge and visually
Set the valve at outlet (flowrate adjustment). Flowrate measurement. Positions of 3-way cocks.
Viscous liquids-driving pressure of compressed air adjustment
Control and Computer (temperature/level/power/ measurement)
Electrical conductivity probes, electronics connection
Disassembly of head, heating tank and electrodes
Assembly of electrodes and heating tank
Assembly of head (power and temperature)

Circuit diagrams and GEOMETRY

Source and control Power control Temperature (Pt100)
Power sockets Connectors to PC (upgrades) Conductivity (connectors and diagrams)

OHMICAS and PCL818 -programs for monitoring T,P,V,C

Program OHMICAS displays and records data from max.16 channels of A/D PCL 818 card (Single Ended analog inputs). Channels 1-6 are temperatures [C] (tank from bottom to head), 7 electrical power [kW], 8 liquid level [litres], 9-11 temperatures [C] (inlet temperature in head and temperatures in tanks), 12-15 conductivities, and channel 16 is auxiliary. Voltage (in the range +-10 V) is converted to physical quantities by linear transformation.
OHMICAS1 OHMICAS2You can have this program in executable form OHMICAS.EXE, or a source form OHMICAS.FOR.
PCL818-measurement PCL818-RTD identification A new development is program PCL818 PCL.ZIP (source and exe) Modified 23.5.2001, which controls two PCL818 cards (32 channels) at base addresses 300H, 310H. Quadratic transformation of acquired data can be adjusted interactively. A new algorithm for simultaneous calibration (Word-7 [140KB]) of several thermocouples is implemented. Also a new algorithm for deconvolution (Word 40kB) has been implemented.

OHN -numerical solution of temperature field (perforated electrodes)

Program OHN solves 2D distribution of temperatures by Control Volume method. Density is assumed constant, this is oversimplification.
ohn-isotherms ohn-full isotherms You can have this program in executable form OHN.EXE, or a source form OHN.FOR.

CVASYM -asymmetry of temperature field (perforated electrodes)

Natural convection. Integral model. Suitable for prediction of influence of viscosity, power, and first of all geometry (width of lateral channels, geometry of perforation) upon asymmetry of flow in lateral channels, and cross-flow through perforation. All properties are constant, except specific electrical conductivity and density. RTD model is included - results were compared with measurement by KCl and TC99 (presented at RCA IAEA Prague November 2000).
cvasym-instab cvasym-instab1 You can have this program in executable form CVASYM.EXE, or a source form CVASYM.FOR.

Calibration (graphs and equations)

Liquid level (August 98) Pt100 (September 99) Power (September 99)
T1 (bottom) T2 T3
T4 T5 (top) T6 (outlet)
T1-T6,TC,PT3,4(Jan.2001) Coeffs A,B,C(Jan.2001)
Thermometers (Testo945,Ama,M3860M,Infrared) Excel sheet (tested December 99)
Calibration of Pt100| Time constant by M.Novy (2000)
Delta probe - Hanna graph (October 2000)

Source data (data acquisition PCL818)

Date Description Source files (OUT,TXT) RTD or XLS files Video/graph
May 2001 full electrodes, water, H=18mm 0805_txt.zip 1805_txt.zip 1905_txt.zip 2105_txt.zip asymetric001.xls mmddhhmm.mpg

Numerical simulation (COSMOS)

Date Description Source file (SES,GEO) Results (OUT) Graphs
may 2001 mmddhhmm.geo mmddhhmm.out mmddhhmm.gif

Numerical simulation (FLUENT)

Date Description Source file (CAS) Results (OUT) Graphs
2001 mmddhhmm.cas mmddhhmm.out mmddhhmm.gif

Numerical simulation (CV-ASYM)

Date Description Source file (DAT) Results (OUT) Graphs
2001 mmddhhmm.dat mmddhhmm.out mmddhhmm.gif

Accessories (universal instruments)

Conductivity (Hanna HI 9635) WTW InoLab Multi L3 (conductivity /Tetracon, Tetracon S/,pH /Sentix/, Ox /CellOx/) Balances Scaltec SAC72, HF2000G M3860 - power and temperature measurement (small batch heater)
pH Scan 3 AMA digit (thermometer) Testo 945 (2 channel thermometer) Testo IR Infrared thermometer

Upgrades of instruments September 2000

MIC2000 (10xPt100) Overall view EA 4000/4.5 - universal power source Thermostat Lauda 203
GNS-data logger, Robotron 20046 Batch Nortech Reflex TS-RX4-FL (4xTP-21-M02 optical probes) WTW Inolab Multi Level 3 SET
Transversing thermocouple Data Acquisition/Switch Unit 34970A, 20 channel multiplexer 34901A Refrigerator Gorenje and MW oven 800W Infrared keyboard (for improved control of continuous and batch heaters)

Capillary viscometer (by product of tracer injection monitoring by a pressure transducer)

  • Syringe (10ml) and needles
  • XTM-190M, 9V battery
  • PCLD-8115, 818L
Kulite XTM-190M 4-wires:
Red,Black(battery),Green,White(A/D card).
Output 75mV/full range
Start program VISCOM. Select needle according to viscosity, and treshold of Voltage. Program identifies start and end of run automatically.
Inject sample and follow pressure time course. Begin and end of sampling is indicated. If the run was too short (less than 2 s) a message is shown INVALID. Measurement can be repeated several times and basic statistics are shown: mean viscosity, estimated error, range of shear rates, max.Reynolds number. Kulite specification, needles selection.
Screen during measurement [F10]-rheograms Viscosity range can be estimated for a selected needle using Excel sheet.
You can have software VISCOM.EXE in executable, VISCOM.FOR or a source form.

Properties of processed materials




@TEC: 3. 3.2003 Change language to English DEFAULT BACKpeoples U218 FS-CVUT Interesting links mailto: Zitny